Yes, the lab protocol it actually suggests would likely lead to an explosion and injury to the operator. Mixing sodium metal and a reagent and adding heat does not usually end well unless/even done under an inert atmosphere (nitrogen or argon).. Also there is no mention of a “work-up step,“ which here would usually involves careful quenching with ethanol necessary to remove residual reactive sodium, and then shaking with an aqueous base.
Yes, the lab protocol it actually suggests would likely lead to an explosion and injury to the operator. Mixing sodium metal and a reagent and adding heat does not usually end well unless/even done under an inert atmosphere (nitrogen or argon).. Also there is no mention of a “work-up step,“ which here would usually involves careful quenching with ethanol necessary to remove residual reactive sodium, and then shaking with an aqueous base.